Synthesis,extraction, and adsorption properties of calix[4]arene‐poly(ethylene‐glycol) crosslinked polymer

Novel calix[4]arene‐poly(ethylene glycol) crosslinked polymer (CCP) has been synthesized by the polycondensation reaction between a p‐tert‐butylcalix[4]arene derivative and dihydroxyl capped poly(ethylene glycol) (DHPEG, M_n = 1000) catalyzed by neodymium tosylate. The hydrogel, consisted of 66.9% water and 33.1% CCP, can selectively extract aromatic organic molecules from aqueous solution according to the diameter of the guest molecules, which infers that the diameter of the calix[4]arene cavity is about 5.4 Å and the conformation of calix[4]arene units altered from cone conformation to 1,3‐alternate conformation during the polycondensation reaction. Furthermore, CCP can also adsorb naphthalene from gas phase, showing much higher capacity than active carbon does, which may have some potential applications in the field of separation and environment protection. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008     

Potential applications of poly(vinyl alcohol)‐congo red aqueous solutions and hydrogels as liquids for hydraulic fracturing

The authors report on the viscoelastic characterization of guar hydrogels obtained through complexation reactions with borax ions. These gels are compared with hydrogels obtained from poly(vinyl alcohol) of different degree of hydrolysis through complexation reactions with congo red. The effect of the degree of hydrolysis and both, the concentration of PVA and the concentration of congo red, on the viscoelastic properties of the hydrogels is analyzed. The potential use of the PVA‐based hydrogels as hydraulic fracturing liquids is discussed in relation to the commonly used fracturing liquid based on the guar–borax system. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008     

啤酒中测定双乙酰含量的EBC法的改进

EBC法是测定啤酒双乙酰的常规方法,但大量报道此法再生性和重复性较差,本文对影响此方法的一些因素进行了考查,发现酸碱度是影响EBC法的一个重要因素,并对EBC法进行改进。     

偏振CARS研究核苷分子振动结构

用偏振灵敏ＣＡＮＳ光谱研究尿嘧啶、胸腺嘧啶、胞嘧啶和腺嘌呤四种核苷分子的振动结构。谱的非共振背景被有效地消除，核苷的双键振动模清晰可辨，对每种核苷分子的特征谱线进行了标识，作为在生物分子中识别它们的标志。     

二次开发WinCC嵌入模糊控制算法

介绍了WinCC(WindowsControlCenter)的基本功能 ,详细阐述了如何利用WinCC的全局脚本编辑器 ,将用户自行开发的模糊控制算法嵌入WinCC中。通过WinCC与PLC之间的通讯 ,实现对某污水处理装置pH值的模糊控制     

可燃气体检测报警系统的分析和检修

分析可燃气体检测报警系统的组成和检修方法，并列举了根据故障现象进行分析和检修的实例。     

电荷灵敏放大器不用反馈高值电阻的新方法

本文提出了一种电荷灵敏放大器不用反馈高值电阻的新方法。对这种方法作了电路分析以及对实际电路的测量结果作了介绍。     

Role of pH and Ionic Strength on Water Relationships in Washed Minced Chicken-breast Muscle Gels

ABSTRACT The relationship between pH, ionic strength, and water balance of chicken-breast muscle gels was investigated. An increase in gel pH (pH 6.4 to 7.4) without added NaCl led to dramatic increases in water-holding capacity and water uptake (P < 0.05). Gels at 150 mM NaCl exhibited less ability to adsorb water than salt-free gels (P < 0.05 at pH 6.8 to 7.4) and had lower water-holding capacities (P < 0.05) and fold scores at and below pH 7. Varying salt concentration of the gel-bathing solutions had dramatic effect on the water uptake of the gels. The results show that strong water-absorbing gels can be produced at low ionic strengths and suggest that the negative charge of the muscle proteins is the driving force for water uptake and retention.     

坐标测量机激光非接触式测头的研制

本文介绍适用子精密大型测试仪器──坐标测量机的激光非接触式测头的研制。该测头采用ＰＳＤ作为敏感元件并采用单片机技术完成对测量数据的处理。     

DKNNS:面向延迟敏感型应用的可扩展精确分布式K近邻搜索算法研究

为了降低用户访问延迟,延迟敏感型网络应用需要选择合适的邻近服务节点响应用户访问请求.分布式K近邻搜索通过可扩展的选择距任意用户节点邻近的K个服务节点,可以有效满足网络应用延迟优化的目的.已有工作在精确度以及可扩展性等方面存在不足.针对可扩展精确的K近邻搜索问题,文中提出了分布式K近邻搜索方法DKNNS(distributed K nearest neighbor search).DKNNS将大量的服务节点组织为邻近性感知的多级环,通过最远节点搜索机制选择优化的K近邻搜索初始化节点,然后基于回退方式快速的在目标节点邻近区域发现K个近邻.基于理论分析,模拟测试以及真实环境下的部署实验发现,在不同规模的节点集合下,DKNNS算法能够确定近似最优的K个服务节点.且DKNNS的查询延迟,查询开销均显著低于Meridian算法.最后,DKNNS的返回结果相对于Meridian具有较高的稳定性.